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HRID986655

反应详情

EQUATION

反应方程式

HRID 986655 的结构方程式

REACTANTS

反应物

2
结构：CCOCC.FB(F)F
HCID8000

Ethane, 1,1'-oxybis-, compd. with trifluoroborane (1:1)

C4H10BF3O

结构：Cc1cc(F)ccc1NC(=O)c1cc([N+](=O)[O-])ccc1NC(=O)CF
HCID13376458

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(F)ccc1-n1c(CF)nc2ccc([N+](=O)[O-])cc2c1=O
HCID13376466

未命名化合物

收率 79.1%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

4.0 g of N-(2-fluoroacetamido-5-nitrobenzoyl)-2-methyl-4-fluoraniline, 3.5 g of boron trifluoride etherate and 30 ml of acetic acid are treated in the same manner as described in Example 1-(2), whereby 3.0 g of 2-fluoromethyl-3-(2-methyl-4-fluorophenyl)-6-nitro-4(3H)-quinazolinone are obtained as colorless prisms.