HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 15228813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 4-tert-Butyl 1-methyl 2-methylidenebutanedioate | HCID 18173165 | — |
| Reactant | HCID 19880118 | HCID 19880118 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15228813 | HCID 15228813 | — |
Reaction Steps
By methods used in Example 2 and employing methyl-2-t-butoxycarbonylmethylacrylate was prepared methyl-1-benzyloxycarbonylaminoethyl-[2-carbomethoxy-3-butoxycarbonyl-1-propyl]phosphinate. TLC (silica, 9:1, ethyl acetate:acetonitrile) Rf =0.58.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04715994 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-161b50b882f045bea1588105b1a79904 |
| Source note | uspto-grants-1987_12 |