HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86741952, compound → HCID 55283956, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86741952 | HCID 86741952 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 55283956 | HCID 55283956 | — |
Reaction Steps
A 10 g portion of 3,4-diazido-2,3,4-trideoxy-D-erythro-pentitol, dibenzeate was dissolved in 35 ml of ethanol, a 1.8 g portion of platinum dioxide added and the mixture reduced in a Parr shaker overnight. The catalyst was removed by filtration and the filtrate evaporated to dryness, giving 4.36 g of 3,4-diamino-2,3,4-trideoxy-D-erythro-pentitol, 1,5-dibenzerate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04716157 |
| Source dataset | uspto-grants-1987_12 |
| ORD ID | ord-6b5275caae7b4f768758f2852e1d84e3 |
| Source note | uspto-grants-1987_12 |