Water → HCID 22988144, compound

Participants

Reaction Steps

5.9 g (26 mmol) of naphthalene-2-sulfonyl chloride were added in portions at room temperature to 4.7 g (25 mmol) of methyl 6-aminonicotinate hydrochloride in 100 ml of dry pyridine. The entire mixture was then stirred at room temperature for 16 h. The reaction solution was then poured onto 500 ml of water and the precipitate obtained was filtered off with suction. 6.4 g (75%) of the product were obtained.

Provenance & Evidence