2-Bromomethylnaphthalene → HCID 22988110, compound

HRID 987068Notes

Reaction equation

HRID 987068 reaction equation
[NH:1]1[CH:5]=[CH:4][N:3]=[C:2]1[C:6]([O:8][CH2:9][CH2:10][CH2:11][CH3:12])=[O:7].Br[CH2:14][C:15]1[CH:24]=[CH:23][C:22]2[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=2)[CH:16]=1>>[CH:16]1[C:17]2[C:22](=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH:23]=[CH:24][C:15]=1[CH2:14][N:1]1[CH:5]=[CH:4][N:3]=[C:2]1[C:6]([O:8][CH2:9][CH2:10][CH2:11][CH3:12])=[O:7]

Participants

3

Reactant 2

HCID 703202-BromomethylnaphthaleneHCID 22988127HCID 22988127, compound

Product 1

HCID 22988110HCID 22988110, compoundYield 71%

Procedure

5.0 g (29.7 mmol) of butyl imidazole-2-carboxylate and 6.6 g (29.7 mmol) of 2-bromomethylnaphthalene were reacted analogously to procedure 8a. 6.4 g (71%) of the product were obtained.

Sources & evidence

ORD record
ord-8c1c78df20dc4e6386cfc9d4162e928d
Source dataset
uspto-grants-2003_10
Patent number
US06630493B1

Reaction notes

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