HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131724087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178453514 | HCID 178453514 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 131724087 | HCID 131724087 | — |
Reaction Steps
3.1 g (10.5 mmol) of [3-[N-(tert-butoxycarbonyl)amino]propyl]-N-(bromoacetyl)-amide (Example 49a) is stirred with 50 mmol. of 1M hydrochloric acid in ethyl acetate for five hours at room temperature. The product is suctioned off, and the solid is rewashed with ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06630570B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-2439a741cfd44b979bd95732e1e0321b |
| Source note | uspto-grants-2003_10 |