HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Benzyloxyphenyl)-2-methoxypropanoic acid methyl ester → Methyl 3-(4-hydroxyphenyl)-2-methoxypropanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Benzyloxyphenyl)-2-methoxypropanoic acid methyl ester | HCID 12616041 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 3-(4-hydroxyphenyl)-2-methoxypropanoate | HCID 10965756 | 87% |
Reaction Steps
3-(4-Benzyloxyphenyl)-2-methoxypropanoic acid methyl ester (1.91 g; 6.36 mmole) was hydrogenated in methanol (30 ml) using Pd/C (5%, wet, 0.9 g) as catalyst. The mixture was filtered through celite and the filtrate was evaporated in vacuo to give 1.16 g (yield 87%) of 3-(4-hydroxyphenyl)-2-methoxypropanoic acid methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06630600B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-1c9d470edc554c7aa88194000e7fb9be |
| Source note | uspto-grants-2003_10 |