Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Methyl 3-oxovalerate | HCID 121699 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Methyl 3-aminopent-2-enoate | HCID 57860398 | — |
Reaction Steps
Methyl 3-oxopentanoate (10 g, 77 mmol) was treated with 2M ammonia in ethanol (200 mL), heated at 80° C. in a sealed tube for 16 hours and concentrated to dryness to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06632418B2 |
|---|
| Source dataset | uspto-grants-2003_10 |
|---|
| ORD ID | ord-518da671a7264f91a9464ab472c00381 |
|---|
| Source note | uspto-grants-2003_10 |
|---|
