HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isocyanate → HCID 178465301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | HCID 178508149 | HCID 178508149 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178465301 | HCID 178465301 | — |
Reaction Steps
To a solution of 7 (40 mg, 0.19 mmol) in THF (1 mL) was added ethyl isocyanate (27 μL, 0.34 mmol) as a solution in THF (0.5 mL). The reaction was heated to reflux overnight then concentrated in vacuo. The crude product was purified by preparative HPLC to afford Ia-84.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632809B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-b2dbc2836e5443b5bb2b2275fc41eaca |
| Source note | uspto-grants-2003_10 |