HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-(5,6,7-trimethoxynaphthalen-2-yl)propenoate → Ethyl 3-(5,6,7-trimethoxynaphthalen-2-yl)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-(5,6,7-trimethoxynaphthalen-2-yl)propenoate | HCID 68436859 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Ethyl 3-(5,6,7-trimethoxynaphthalen-2-yl)propionate | HCID 21891562 | — |
Reaction Steps
Ethyl 3-(5,6,7-trimethoxynaphthalen-2-yl)propenoate (1.70 g) was dissolved in methanol (20 mL), 10% palladium on carbon (510 mg) was added to the solution, and the mixture was stirred at room temperature for 2.5 hours under a hydrogen atmosphere. The reaction mixture was filtered, and the filtrate was then concentrated to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632810B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-5521fe97ec2940168d1d875d1077ade8 |
| Source note | uspto-grants-2003_10 |