HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 15294258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Isopropyl-3-methylsulfonylbenzoic acid | HCID 10633915 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15294258 | HCID 15294258 | — |
Reaction Steps
4.0 g of 3-methylsulfonyl-4-i-propylbenzoic acid, 1.5 ml of thionyl chloride and 3 drops of DMF are heated under reflux for 10 h in 30 ml of toluene. The solvent is subsequently removed in vacuo and the product is taken for further use without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632840B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-eee581ab9e714f7f869a7ee3668cca98 |
| Source note | uspto-grants-2003_10 |