HuagongsheHuagongshe Chemistry Print Report · For research reference only
3(E)-[4-Ethoxy-3-Propoxyphenyl]Acrylic Acid → HCID 22987079, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3(E)-[4-Ethoxy-3-Propoxyphenyl]Acrylic Acid | HCID 17775576 | — |
| Solvent | Toluene ethylacetate | HCID 21584019 | — |
| Product | HCID 22987079 | HCID 22987079 | — |
Reaction Steps
The preparation is carried out analogously to Example 1 from 1.0 g (4.00 mmol) of 3(E)-[4-ethoxy-3-propoxyphenyl]acrylic acid and 0.92 g (4.39 mmol) of 8-bromo-1-hexanol and, according to chromatography over 150 g of silica gel using toluene/ethyl acetate, gives 8-hydroxyoctyl 3(E)-[4-ethoxy-3-propoxyphenyl]acrylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632909B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-2a9110554822438e8b189f15aec5e95f |
| Source note | uspto-grants-2003_10 |