HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butyloxy-3,5-di-tert-butylphenylboronic acid → 3-(3',5'-di-tert-butyl-6-hydroxy-2'-butyloxy-3-biphenylyl)acrylic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butyloxy-3,5-di-tert-butylphenylboronic acid | HCID 22345412 | — |
| Reactant | Ethyl 3-(3-bromo-4-hydroxyphenyl)acrylate | HCID 69793988 | — |
| Product | 3-(3',5'-di-tert-butyl-6-hydroxy-2'-butyloxy-3-biphenylyl)acrylic Acid | HCID 69792688 | 7.2% |
Reaction Steps
In a manner similar to that of Example 1(c), by reaction of 6.2 g (22.8 mmol) of ethyl 3-(3-bromo-4-hydroxyphenyl)acrylate obtained in Example 34(d) with 14 g (45.7 mmol) of 2-butyloxy-3,5-di-tert-butylphenylboronic acid obtained above, 700 mg (7%) of the expected compound were obtained in the form of a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632963B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-d1b56e3bb4964a83b2daccea9360f228 |
| Source note | uspto-grants-2003_10 |