Benzaldehyde → HCID 131724099, compound

HRID 988066Notes

Reaction equation

HRID 988066 reaction equation
[CH2:1]([NH2:7])[CH2:2][O:3][CH2:4][CH2:5][OH:6].[CH:8](=O)[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>O>[CH2:1]([NH2:7])[CH2:2][O:3][CH2:4][CH2:5][OH:6].[CH:8](=[NH:7])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

Participants

4

Reactant 2

HCID 240BenzaldehydeHCID 13578Diglycolamine

Product 1

HCID 131724099HCID 131724099, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Diglycolamine (1000.9 g) and benzaldehyde (1060.7 g) were heated under vacuum at 95° C. until the % water was less than 0.1% to yield the diglycolamine-benzaldehyde imine.

Sources & evidence

ORD record
ord-dc5d1cfaab2a408abff8c9c5e6929a7d
Source dataset
uspto-grants-2003_10
Patent number
US06635350B2

Reaction notes

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