HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenylpiperazine → 2,7-Bis-[3-(4-phenyl-piperazin-1-yl)propionyl]-xanthene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenylpiperazine | HCID 7096 | — |
| Reactant | 2,7-Bis(3-chloropropionyl)xanthene | HCID 12340279 | — |
| Product | 2,7-Bis-[3-(4-phenyl-piperazin-1-yl)propionyl]-xanthene | HCID 10121739 | — |
Reaction Steps
Prepared from compound 17 and 4-phenyl-piperazine according to General Procedure C to give a solid. Mp 206-208° C. 1H NMR (CDCl3, 400 MHz) δ7.91-7.86 (m 4H), 7.29 (t, J=10 Hz, 4H), 7.14 (d, J=10 Hz, 2H), 6.96-6.91 (m, 6H), 4.16 (s, 2H), 3.51-3.46 (m, 12H), 3.38-3.10 (m, 12H). Anal. (C39H42N4O3.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06635786B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-bdbfa8efd9974e3ba4131474d38c92b9 |
| Source note | uspto-grants-2003_10 |