HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 11514448, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Reactant | 5-Fluoro-2-nitrotoluene | HCID 94956 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 11514448 | HCID 11514448 | — |
Reaction Steps
A mixture of 31.2 g (0.2 mol) of 4-fluoro-2-methyl-1-nitrobenzene, 37.5 g (0.3 mol) of 3-imidazol-1-ylpropylamine and 34.8 ml (0.25 mol) of triethylamine in 30 ml of 1,2-dimethoxyethane was heated with stirring for 3 hours on a boiling water bath.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638321B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-bf40319dd25340ba85eb71cf9be17ffa |
| Source note | uspto-grants-2003_10 |