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HRID988922

反应详情

EQUATION

反应方程式

HRID 988922 的结构方程式

REACTANTS

反应物

2
结构：Cn1ccnc1
HCID1390

1-Methylimidazole

C4H6N2

结构：O=[N+]([O-])c1ccc(O)c(CCl)c1
HCID76305

Phenol, 2-(chloromethyl)-4-nitro-

C7H6ClNO3

PRODUCTS

生成物

1
结构：Cn1cc[n+](Cc2cc([N+](=O)[O-])ccc2O)c1.[Cl-]
HCID178480833

未命名化合物

PROCEDURE

实验过程

Starting with 56.3 g (0.3 mol) of 2-chloromethyl-4-nitrophenol and 29.6 g (0.36 mol) of 1-methyl-1H-imidazole, 65.1 g of yellow crystals melting with decomposition at 250-260° C. (Kofler) were obtained, the elemental analysis of which, calculated for C11H12N3O3Cl, was:

WORKUP

后处理

  1. custommelting with decomposition at 250-260° C.
  2. customwere obtained