HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 2-aminoisobutyrate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Aminoisobutyric acid | HCID 6119 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Methyl 2-aminoisobutyrate hydrochloride | HCID 13258034 | 97.4% |
Reaction Steps
This was synthesised according to Standard Procedure 1, using 2-amino-isobutyric acid (4 g, 0.039 mol) with thionyl chloride (5.66 ml, 0.078 mol) and anhydrous methanol (23.5 ml, 0.58 mol). This gave the product as a white solid (5.805 g, 97.4%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638919B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-dd5d06c2ffff4c789cbefa6557f8ad32 |
| Source note | uspto-grants-2003_10 |