HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopyrimidine → HCID 9861826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopyrimidine | HCID 7978 | — |
| Reactant | 5-(Methylsulfanyl)thiophene-2-carbaldehyde | HCID 2736997 | — |
| Reactant | HCID 86587200 | HCID 86587200 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | HCID 9861826 | HCID 9861826 | — |
Reaction Steps
Compound (26) was prepared in accordance with general instructions 1 from 1.0 ml 2-aminopyrimidine solution (0.1 M, MC), 0.575 ml tert-butylisonitrile isocyanide solution (0.2 M, MC), 0.500 ml 5-methylsulfanyl-thiophene-2-carbaldehyde solution (0.3 M, MC), and 10 μl perchloric acid (w=20%). Calculated mass 318.5; found mass 319.2 (ESI-MS)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638933B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-9ed0afd657274934b001bb3cfaa9a5e3 |
| Source note | uspto-grants-2003_10 |