HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopyridine → HCID 18004783, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Reactant | Cyclohexyl isocyanide | HCID 79129 | — |
| Reactant | 3-Bromothiophene-2-carboxaldehyde | HCID 2797079 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | HCID 18004783 | HCID 18004783 | — |
Reaction Steps
Compound (27) was prepared in accordance with general instructions 1 from 1.0 ml 2-aminopyridine solution (0.1 M, MC), 0.575 ml cyclohexyl isocyanide solution (0.2 M, MC), 0.500 ml 3-bromothiophene-2-carbaldehyde solution (0.3 M, MC), and 10 μl perchloric acid (w=20%). Calculated mass 376.3; found mass 376.4/378.3 (ESI-MS)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638933B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-d11e78407fb14760bef3fa8891cb2269 |
| Source note | uspto-grants-2003_10 |