HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopyrimidine → HCID 18004778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopyrimidine | HCID 7978 | — |
| Reactant | 1,1,3,3-Tetramethylbutyl isocyanide | HCID 26725 | — |
| Reactant | 2-Chloro-4-fluorobenzaldehyde | HCID 145024 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | HCID 18004778 | HCID 18004778 | — |
Reaction Steps
Compound (29) was prepared in accordance with general instructions 1 from 1.0 ml 2-aminopyrimidine solution (0.1 M, MC), 0.575 ml 1,1,3,3-tetramethylbutyl isocyanide solution (0.2 M, MC), 0.500 ml 2-chloro-4-fluorobenzaldehyde solution (0.3 M, MC), and 10 μl perchloric acid (w=20%). Calculated mass 374.9; found mass 375.3 (ESI-MS)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638933B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-167e355bad2142b9abcca835bc40bc87 |
| Source note | uspto-grants-2003_10 |