HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthaldehyde → HCID 9818341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthaldehyde | HCID 6195 | — |
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Reactant | Tert-Butyl isocyanide | HCID 23577 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | HCID 9818341 | HCID 9818341 | — |
Reaction Steps
Compound (31) was prepared in accordance with general instructions 1 from 1.0 ml 2-aminopyridine solution (0.1 M, MC), 0.575 ml tert-butyl isocyanide solution (0.2 M, MC), 0.500 ml naphthalene-1-carbaldehyde solution (0.3 M, MC), and 10 μl perchloric acid (w=20%). Calculated mass 315.4; found mass 316.3 (ESI-MS)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638933B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-e8286fa03dc14a53a0cbe72b87e2192e |
| Source note | uspto-grants-2003_10 |