Sodium Iodide → HCID 22719916, compound

HRID 989064Notes

Reaction equation

HRID 989064 reaction equation
F[P-](F)(F)(F)(F)F.[CH3:8][N+:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[CH2:15][C:16]([C:18]1[CH:23]=[CH:22][C:21]([CH3:24])=[CH:20][CH:19]=1)=[O:17].[Na+].[I-:26]>CC(C)=O>[I-:26].[CH3:8][N+:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[CH2:15][C:16]([C:18]1[CH:19]=[CH:20][C:21]([CH3:24])=[CH:22][CH:23]=1)=[O:17]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 15487510HCID 15487510, compound

Product 1

HCID 22719916HCID 22719916, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

10 mmol of the compound obtained in Example 1 are dissolved in 35 ml of acetone, and 15 mmol of NaI are added in portions of 100 mg. A white precipitate is obtained immediately and the mixture is stirred for 14 hours in a sealed tube at ambient temperature. The white solid obtained is filtered off and washed with acetone.

Workup

  1. customA white precipitate is obtained immediately
  2. customThe white solid obtained
  3. filtrationis filtered off
  4. washwashed with acetone

Sources & evidence

ORD record
ord-fb0158196cdf458cb89b2d64bec71daa
Source dataset
uspto-grants-2003_10
Patent number
US06638946B2

Reaction notes

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