HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methoxy-6-(trifluoromethyl)indoline → HCID 10767350, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methoxy-6-(trifluoromethyl)indoline | HCID 11206713 | — |
| Reactant | HCID 18005096 | HCID 18005096 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 10767350 | HCID 10767350 | 198.9% |
Reaction Steps
The title compound (0.74 g, 47%) was prepared as an off white solid using the methodology of example 28, with phenyl N-(5-phenyl-3-(pyrid-3-yl)phenyl)carbamate (D31) (0.27 g, 0.76 mmol) and 5-methoxy-6-trifluoromethyl indoline (D11) [0.182 mg, 0.83 mmol] in DMF (10 ml). Melting point: 150°-151° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638953B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-7414e02a6cf7406889a98a5594f8069f |
| Source note | uspto-grants-2003_10 |