HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → 1-[4-(3,5-Dichloro-phenoxy)-benzyl]-pyrrolidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 4-(3,5-Dichlorophenoxy)benzaldehyde | HCID 16244087 | — |
| Product | 1-[4-(3,5-Dichloro-phenoxy)-benzyl]-pyrrolidine | HCID 9836836 | — |
Reaction Steps
The title compound was prepared starting from 4-(3,5-dichloro-phenoxy)-benzaldehyde and pyrrolidine by the same method (step B) described in Example 1. 1H NMR (400 MHz, CDCI3)δ7.22 (t, J=7.8 Hz, 1 H), 7.07 (d, J=7.6 Hz,1 H), 6.96 (m, 2 H), 6.81 (m,1 H), 6.76 (m, 2 H), 3.52 (s, 2 H), 2.45 (m, 4 H), 1.70 (m, 4 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638967B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-8be90798025a4f9eb3529acf116cd19b |
| Source note | uspto-grants-2003_10 |