HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 16495035, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | {4-[(Pyrrolidin-1-yl)methyl]phenyl}methanol | HCID 16495034 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 16495035 | HCID 16495035 | — |
Reaction Steps
A solution of the product of Step C in DCM (200 mL) was treated with thionyl chloride (20 mL) at 40° C. for 16 hours. Solvent was removed in vacuo to give the titled compound (15 g), which was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638967B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-c2fe768ad721481a83c81c09dfad51ef |
| Source note | uspto-grants-2003_10 |