3-Pyridinecarboxaldehyde → HCID 131723530, compound

HRID 989675Notes

Reaction equation

HRID 989675 reaction equation
[CH:1](=O)[C:2]1[CH:7]=[CH:6][CH:5]=[N:4][CH:3]=1.[ClH:9].NC(CS)C[N:13]1[C:19]2[CH:20]=[CH:21][C:22]([C:24]3[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=3)=[CH:23][C:18]=2[CH2:17][N:16]([C:30]([C:32]2[C:41]3[C:36](=[CH:37][CH:38]=[CH:39][CH:40]=3)[CH:35]=[CH:34][CH:33]=2)=[O:31])[CH2:15][CH2:14]1>>[ClH:9].[C:32]1([C:30]([N:16]2[CH2:17][C:18]3[CH:23]=[C:22]([C:24]4[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=4)[CH:21]=[CH:20][C:19]=3[N:13]([CH2:1][C:2]3[CH:3]=[N:4][CH:5]=[CH:6][CH:7]=3)[CH2:14][CH2:15]2)=[O:31])[C:41]2[C:36](=[CH:37][CH:38]=[CH:39][CH:40]=2)[CH:35]=[CH:34][CH:33]=1

Participants

3

Reactant 2

HCID 103713-PyridinecarboxaldehydeHCID 131723531HCID 131723531, compound

Product 1

HCID 131723530HCID 131723530, compound

Procedure

The title compound was prepared from nicotinaldehyde and the compound E of Example 2 by following the procedure described for the preparation of Example 6. MS (M+H): 470.

Workup

  1. customdescribed for the preparation of Example 6

Sources & evidence

ORD record
ord-5112965d12e448c6b00fdcaf36b53a13
Source dataset
uspto-grants-2002_10
Patent number
US06458783B1

Reaction notes

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