Pentylamine → HCID 12043758, compound

Participants

Reaction Steps

A mixture of 4-chloro-5-hexyl-6-methylpyrimidine-2-ylamine (1.00 mg, 0.44 mmol) and amylamine (2 ml) was refluxed for 11 hours. The reaction mixture was cooled and the solvent was removed in vacuo. The residue was purified by silica gel column chromatography (MeOH:CHCl3=1:20) to give the object compound (107 mg, 87%) as an oil.

Provenance & Evidence