HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentylamine → HCID 12043759, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentylamine | HCID 8060 | — |
| Reactant | HCID 22313253 | HCID 22313253 | — |
| Product | HCID 12043759 | HCID 12043759 | 59% |
Reaction Steps
A mixture of 4-chloro-7,8-dihydro-5H-pyrano[4,3-d]pyrimidine-2-ylamine (29.3 mg, 0.158 mmol) and amylamine (1.0 ml) was refluxed for 2.5 hours. After reaction, the procedure according to pro-treatment of Example 7 was carried out to give the object compound (22.3 mg, 59%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06458798B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-ea9967d56962415795864ef0bea23854 |
| Source note | uspto-grants-2002_10 |