Phosphorus oxychloride → HCID 22313241, compound

HRID 989716Notes

Reaction equation

[NH2:1][C:2]1[N:7]=[C:6](O)[C:5]([CH3:9])=[C:4]([CH2:10][CH2:11][CH2:12][CH3:13])[N:3]=1.P(Cl)(Cl)([Cl:16])=O>>[CH2:10]([C:4]1[C:5]([CH3:9])=[C:6]([Cl:16])[N:7]=[C:2]([NH2:1])[N:3]=1)[CH2:11][CH2:12][CH3:13]

Participants

Reactant 2

HCID 24813Phosphorus oxychloride

HCID 178441831HCID 178441831, compound

Product 1

HCID 22313241HCID 22313241, compound

Procedure

By reacting 2-amino-6-butyl-5-methylpyrimidine-4-ol (0.82 g, 4.52 mmol) and phosphorous oxychloride (10 ml), there was obtained the object compound (720 mg).

Sources & evidence

ORD record: ord-b2887b0a8662487982e7e0c84b28985f
Source dataset: uspto-grants-2002_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06458798B1

Reaction notes

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