Methanesulfonyl chloride → HCID 18419552, compound

HRID 989890Notes

Reaction equation

HRID 989890 reaction equation
[C:1]([C:5]1[CH:6]=[C:7]([CH:24]=[C:25]([C:28]([CH3:31])([CH3:30])[CH3:29])[C:26]=1[OH:27])[CH2:8][N:9]([C:18]1[CH:19]=[N:20][CH:21]=[CH:22][CH:23]=1)[S:10]([C:13]1SC=CC=1)(=[O:12])=[O:11])([CH3:4])([CH3:3])[CH3:2].S1C=CC=C1S(Cl)(=O)=O.CS(Cl)(=O)=O>>[C:1]([C:5]1[CH:6]=[C:7]([CH:24]=[C:25]([C:28]([CH3:31])([CH3:30])[CH3:29])[C:26]=1[OH:27])[CH2:8][N:9]([C:18]1[CH:19]=[N:20][CH:21]=[CH:22][CH:23]=1)[S:10]([CH3:13])(=[O:12])=[O:11])([CH3:4])([CH3:3])[CH3:2]

Participants

4

Reactant 3

HCID 31297Methanesulfonyl chlorideHCID 855182-Thiophenesulfonyl chlorideHCID 10276242HCID 10276242, compound

Product 1

HCID 18419552HCID 18419552, compound

Procedure

This compound was prepared in the same manner as for the title compound of Example 7, except the 2-thiophene sulfonyl chloride was replaced with methane sulfonyl chloride. Mp 133—134° C.; MS+1=391.1.

Sources & evidence

ORD record
ord-957009d756654df99ad084dfdb7d77be
Source dataset
uspto-grants-2002_10
Patent number
US06458815B2

Reaction notes

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