HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → HCID 18672845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 18672841 | HCID 18672841 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 18672845 | HCID 18672845 | — |
Reaction Steps
The title compound is prepared according to the procedure of Example 4 from 20 g of the compound of Example 8, 20.4 g of 45% aqueous potassium hydroxide, 10.3 g of thiophenol and 100 g of N-methylpyrrolidone. The title compound is an oil purified by chromatography on silica gel using toluene as eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06458872B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-a736b00a14f64269890b0fbea9f6b6b7 |
| Source note | uspto-grants-2002_10 |