HuagongsheHuagongshe Chemistry Print Report · For research reference only
(+-)-3-Quinuclidinol → 1-(4,6-Diethoxy-1,3,5-triazin-2-yl)-3-hydroxyquinuclidinium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (+-)-3-Quinuclidinol | HCID 15381 | — |
| Reactant | 2-Chloro-4,6-diethoxy-1,3,5-triazine | HCID 35649 | — |
| Product | 1-(4,6-Diethoxy-1,3,5-triazin-2-yl)-3-hydroxyquinuclidinium chloride | HCID 9905579 | — |
Reaction Steps
The operation was carried out in the same manner as in Preparation Example 1 but using 4.07 g (0.02 mols) of a 2-chloro-4,6-diethoxy-1,3,5-triazine and 2.54 g (0.02 mols) of a 3-quinuclidinol to obtain 6.51 g (yield, 98.4%) of white crystals of a 1-(4,6-diethoxy-1,3,5-triazin-2-yl)-3-hydroxyquinuclidinium chloride represented by the following general formula (XII)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06458948B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-df02c8ed69274451bdf10ff233cf0972 |
| Source note | uspto-grants-2002_10 |