Potassium Iodide → HCID 11817999, compound

Participants

Reaction Steps

131.4 g of 2-acetylaminomethyl-4-nitrophenol, 64.4 g of chloroacetamide, 86.4 g of calcium carbonate and 57.1 g of potassium iodide in 800 ml of acetone are heated under reflux for four hours. Subsequently the reaction mixture is cooled to room temperature and poured into 1300 ml of water. The resulting precipitate is filtered, washed with water and subsequently dried. 120 g of a yellow product are obtained having a melting point of from 236 to 240° C.

Provenance & Evidence