Phenethylamine → HCID 10159559, compound

HRID 990717Notes

Reaction equation

[F:1][C:2]([F:23])([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][N:18]=1)[CH2:3][NH:4][C:5]1[C:6](=[O:16])[N:7]([CH2:12][C:13]([OH:15])=O)[C:8]([CH3:11])=[CH:9][N:10]=1.[CH2:24]([NH2:32])[CH2:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1>>[F:23][C:2]([F:1])([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][N:18]=1)[CH2:3][NH:4][C:5]1[C:6](=[O:16])[N:7]([CH2:12][C:13]([NH:32][CH2:24][CH2:25][C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)=[O:15])[C:8]([CH3:11])=[CH:9][N:10]=1

Participants

Reactant 2

HCID 1001Phenethylamine

HCID 10892675HCID 10892675, compound

Product 1

HCID 10159559HCID 10159559, compound

Procedure

8-1 was prepared from [3-(2,2-difluoro-2-pyridin-2-ylethylamino)-6-methyl-2-oxo-2H-pyrazin-1-yl]-acetic acid and phenethylamine essentially according to the procedure of Example 1, Step K. Mass Spectrum: Found: (M+1) 428.2.

Sources & evidence

ORD record: ord-33039162c84f48349fdb1a35245a5687
Source dataset: uspto-grants-2002_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06462050B1

Reaction notes

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