HRID990872
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A mixture of N-(1-naphthalen-2-yl-ethyl)-formamide (1.12 g), ethanol (10 mL) and 5 N sodium hydroxide (10 mL) is heated at reflux for 1 hour. The solution is cooled, poured into water and extracted with ether. The ether solution is dried with anhydrous potassium carbonate, filtered and concentrated to give the product (0.95 g) as a pale yellow oil.
WORKUP
后处理
- temperatureis heated
- temperatureat reflux for 1 hour
- temperatureThe solution is cooled
- extractionextracted with ether
- dry with materialThe ether solution is dried with anhydrous potassium carbonate
- filtrationfiltered
- concentrationconcentrated