HRID990891

反应详情

EQUATION

反应方程式

HRID 990891 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a 0.67 M solution of the benzaldehyde (20.0 mmol) and cyclohexanone (10.0 mmol) in ethanol (15 ml) is added 10 ml 40% KOH at 10° C. After stirring for 12-24 hr at room temperature, the solution is diluted and filtered. The precipitate is recrystallized from ethanol to afford 2,6-dibenzalcyclohexanone and its derivatives.

WORKUP

后处理

  1. additionthe solution is diluted
  2. filtrationfiltered
  3. customThe precipitate is recrystallized from ethanol