HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 53812005, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | N-(1-Oxo-2,3-dihydro-1H-inden-5-yl)acetamide | HCID 312894 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53812005 | HCID 53812005 | — |
Reaction Steps
A mixture of N-(1-oxoindan-5-yl)acetamide (10.0 g, obtained from the Maybridge Chemical Co. Ltd), benzaldehyde (6.73 g), glacial acetic acid (1.06 g) and piperidine (10.8 g) was heated to 90° C. under nitrogen. Methanol (200 ml) was added and the mixture was cooled and then filtered to give N-(2-benzylidene-1-oxo-indan-5-yl)acetamide (13.47 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06462036B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-a7e9ee60c9f1473f8addba167aa7d804 |
| Source note | uspto-grants-2002_10 |