HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 18415810, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 18415841 | HCID 18415841 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18415810 | HCID 18415810 | — |
Reaction Steps
A mixture of ethyl 3-(1,4-dihydroindeno[1,2-c]pyrazol-3-yl)phenoxyacetate (0.66 g), 1M sodium hydroxide solution (4 ml) and ethanol (20 ml) was heated on a steam bath for 30 minutes. The solvent was removed under reduced pressure and the residue was stirred for 1 hour with 1M hydrochloric acid (20 ml) at ambient temperature. The mixture was filtered to give 3-(1,4-dihydroindeno[1,2-c]pyrazol-3-yl)phenoxyacetic acid, m.p. 246-248° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06462036B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-025932611c814feda5357bb7a57b99eb |
| Source note | uspto-grants-2002_10 |