HRID991040
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
2-[4(2-Diethylamino-ethoxy)benzyl]-2-(4-methoxy-benzenesulfonyl)hexanoic acid was prepared starting from 2-[4-(2-diethylamino-ethoxy)benzyl]-2-(4-methoxy-benzenesulfonyl) hexanoic acid ethyl ester (8 g, 15.4 mmol) dissolved in methanol (200 ml) and 10 N NaOH (30 ml). The resulting mixture was worked up as outlined in example 1. Yield 3.88 a crude (51%); brown oil; MS: 492 (M+H)+.
WORKUP
后处理
- customYield 3.88 a crude (51%)