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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 991040Generated: November 1, 2026

HCID 53756990, compound → HCID 18416721, compound

https://huagongshe.com/reaction/991040

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 53756990HCID 53756990—
SolventMethanolHCID 887—
SolventSodium HydroxideHCID 14798—
ProductHCID 18416721HCID 18416721—

Reaction Steps

2-[4(2-Diethylamino-ethoxy)benzyl]-2-(4-methoxy-benzenesulfonyl)hexanoic acid was prepared starting from 2-[4-(2-diethylamino-ethoxy)benzyl]-2-(4-methoxy-benzenesulfonyl) hexanoic acid ethyl ester (8 g, 15.4 mmol) dissolved in methanol (200 ml) and 10 N NaOH (30 ml). The resulting mixture was worked up as outlined in example 1. Yield 3.88 a crude (51%); brown oil; MS: 492 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06462073B2
Source datasetuspto-grants-2002_10
ORD IDord-cb224add9799406ebdefc3650818e3cc
Source noteuspto-grants-2002_10