HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 18416850, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 54443426 | HCID 54443426 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18416850 | HCID 18416850 | 23% |
Reaction Steps
2-[8-(1-Carboxy-ethanesulfonyl)-octane-1-sulfonyl]-propionic acid was prepared according to general method as outline in example 1. Starting from 2-[8-(1-carboxy-ethanesulfonyl)-octane-1-sulfonyl]-propionic acid ethyl ester (3.0 g, 6.8 mmol), ethanol (15 mL) and 10 N sodium hydroxide (15 mL). Yield 2.7 g (98%); white solid mp 99-102° C.; MS 387 (M+NH3)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06462073B2 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-9ed7aaa63c654484b4387d289e354d04 |
| Source note | uspto-grants-2002_10 |