HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Methoxy-phenylsulfanyl)heptanoic acid ethyl ester → HCID 18416776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Methoxy-phenylsulfanyl)heptanoic acid ethyl ester | HCID 54357246 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 18416776 | HCID 18416776 | — |
Reaction Steps
2-(4-Methoxy-phenylsulfanyl)-heptanoic acid was prepared starting with 2-(4-methoxy-phenylsulfanyl)-heptanoic acid ethyl ester (4 g, 13.5 mmol) dissolved in methanol (300 ml) and 10N NaOH (25 ml). The resulting reaction mixture was worked up as outlined in example 1. Yield 3 g (83%). yellow oil. MS: 267.1 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06462073B2 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-42fe8787b9db4d1483389ede32d026a6 |
| Source note | uspto-grants-2002_10 |