Diethanolamine → HCID 11010053, compound

HRID 991099Notes

Reaction equation

HRID 991099 reaction equation
[NH:1]([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4].Cl[CH2:9][CH2:10][C:11]1[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[CH:13][CH:12]=1>>[OH:4][CH2:3][CH2:2][N:1]([CH2:9][CH2:10][C:11]1[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[CH:13][CH:12]=1)[CH2:5][CH2:6][OH:7]

Participants

3

Reactant 2

HCID 8113DiethanolamineHCID 875134-(2-Chloroethyl)phenyl methyl ether

Product 1

HCID 11010053HCID 11010053, compound

Procedure

2-{(2-Hydroxy-ethyl)-[2-(4-methoxy-phenyl)-ethyl]-amino}-ethanol was prepared according to the general method as outlined in example 83. Starting from diethanolamine (10.0 g, excess). and 1-(2-chloroethyl)4-methoxybenzene (8.5 g, 50 mmol). Yield 1 -1 g, (92%); yellow oil; MS: 240 (M+H)+.

Sources & evidence

ORD record
ord-7e19617ecb0844f1806397aa39b2c64b
Source dataset
uspto-grants-2002_10
Patent number
US06462073B2

Reaction notes

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