HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-1,2,4-Triazole → HCID 131723224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-1,2,4-Triazole | HCID 9257 | — |
| Reactant | Distearylmethylamine | HCID 77709 | — |
| Reactant | Tris(pentafluorophenyl)borane | HCID 582056 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 131723224 | HCID 131723224 | — |
Reaction Steps
1,2,4-triazole (0.1349 g, 1.953 mmol), tris(pentafluorophenyl)borane (2.0000 g, 3.9063 mmol) and dioctadecylmethylamine (1.0469 g, 1.9531 mmol) were placed in a 50 mL flask, taken up in 21 mL of toluene and refluxed under argon for 5 hours. The volatiles were then stripped under vacuum. Yield, 2.702 g, 84.92 percent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06462156B2 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-8bc796428a6447a88c999537e1806b39 |
| Source note | uspto-grants-2002_10 |