HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanecarbonitrile, 1-(4-oxo-1-phenyl-1,3,8-triazaspiro(4,5)dec-8-yl)- → HCID 18414048, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanecarbonitrile, 1-(4-oxo-1-phenyl-1,3,8-triazaspiro(4,5)dec-8-yl)- | HCID 3063729 | — |
| Reactant | HCID 178419663 | HCID 178419663 | — |
| Product | HCID 18414048 | HCID 18414048 | 54% |
Reaction Steps
This was prepared according to the procedure described in Example 1 using 1-(4-oxo-1-phenyl-1,3,8-triazaspiro[4.5]dec-8-yl)cyclohexanecarbonitrile instead of 1-(4-oxo-1-phenyl-1,3,8-triazaspiro[4.5]dec-8-yl)cycloheptanecarbonitrile and benzylmagnesium bromide instead of phenylmagnesium bromide. Yield was 54%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06465478B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-7250aba54e984e5f9aa4c30c273f9e75 |
| Source note | uspto-grants-2002_10 |