HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(Propan-2-yl)-2H-1,3-benzodioxol-5-amine → 1-(1,3-Benzodioxol-5-yl)-1-isopropylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(Propan-2-yl)-2H-1,3-benzodioxol-5-amine | HCID 12789466 | — |
| Reactant | HCID 178418852 | HCID 178418852 | — |
| Product | 1-(1,3-Benzodioxol-5-yl)-1-isopropylurea | HCID 100555 | 83% |
Reaction Steps
The title compound was prepared from N-isopropyl-3,4-(methylenedioxy)aniline and NaOCN by the procedure described in example 5 in 83% yield. 1H NMR (CDCl3): 6.85-6.65 (m, 3H), 6.04 (s, 2H), 4.82 (m, 1H), 4.21 (br s, 2H), 1.06 (d, J=6.6, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06465472B1 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-49498f9acb064efabf48cf4af13f3053 |
| Source note | uspto-grants-2002_10 |