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HRID991522

反应详情

EQUATION

反应方程式

HRID 991522 的结构方程式

REACTANTS

反应物

2
结构：CC(C)N(C(N)=O)c1ccc2c(c1)OCO2
HCID100555

1-(1,3-Benzodioxol-5-yl)-1-isopropylurea

C11H14N2O3

结构：O=Cc1cc2c(cc1Cl)OCO2
HCID140014

6-Chloropiperonal

C8H5ClO3

PRODUCTS

生成物

1
结构：CC(C)N1C(=O)NC(c2cc3c(cc2Cl)OCO3)c2cc3c(cc21)OCO3
HCID12150180

未命名化合物

收率 65%

PROCEDURE

实验过程

This compound was synthesized from N-isopropyl-N-[3,4-(methylenedioxy)-phenyl]urea (410 mg) and 6-chloropiperonal (350 mg) by the procedure described in example 10 in 65% yield. 1H NMR (CDCl3): 6.86 (s, 1H), 6.77 (s, 1H), 6.48 (s, 1H), 6.40 (s, 1H), 5.95 (s, 4H), 5.66 (d, J=2.5, 1H), 5.21 (s, 1H), 4.48 (m, 1H), 1.53 (d, J=6.5, 6H).