HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → 4-Cyclohexyl allyloxyphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Cyclohexylphenol | HCID 14327 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 4-Cyclohexyl allyloxyphenol | HCID 18414635 | 94.1% |
Reaction Steps
A solution of 4-cyclohexylphenol (10 g), allyl bromide (13.74 g) and potassium carbonate (9.42 g) in acetone (150 mL) was kept at reflux for 10-12 h. The solution was cooled, filtered and concentrated under reduced pressure to provide 4-cyclohexyl allyloxyphenol (12.4 g). This product was used as such for Step C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06465497B2 |
| Source dataset | uspto-grants-2002_10 |
| ORD ID | ord-9b4675d95fb743ea96381e652fbc95c8 |
| Source note | uspto-grants-2002_10 |