HRID991578

反应详情

EQUATION

反应方程式

HRID 991578 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 4-cyclohexylphenol (10 g), allyl bromide (13.74 g) and potassium carbonate (9.42 g) in acetone (150 mL) was kept at reflux for 10-12 h. The solution was cooled, filtered and concentrated under reduced pressure to provide 4-cyclohexyl allyloxyphenol (12.4 g). This product was used as such for Step C.

WORKUP

后处理

  1. temperatureat reflux for 10-12 h
  2. temperatureThe solution was cooled
  3. filtrationfiltered
  4. concentrationconcentrated under reduced pressure